DR ANTHONY MELVIN CRASTO,WorldDrugTracker, helping millions, A 90 % paralysed man in action for you, I am suffering from transverse mylitis and bound to a wheel chair, With death on the horizon, nothing will not stop me except God................DR ANTHONY MELVIN CRASTO Ph.D ( ICT, Mumbai) , INDIA 25Yrs Exp. in the feld of Organic Chemistry,Working for GLENMARK GENERICS at Navi Mumbai, INDIA. Serving chemists around the world. Helping them with websites on Chemistry.Million hits on google, world acclamation from industry, academia, drug authorities for websites, blogs and educational contribution

Friday 24 July 2015

1,2-Bis(2-aminophenoxy)ethyl-N,N,N',N'-acetic acid methyl ester






http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532014000100014&lng=en&nrm=iso&tlng=en



1,2-Bis(2-aminophenoxy)ethyl-N,N,N',N'-acetic acid methyl ester 4
Compound 3 (2.44 g, 0.01 mol) was dissolved in MeCN (10 mL), then (i-Pr)2NEt (6 mL) and methyl bromoacetate (3 mL) were added to the mixture with stirring. The reaction mixture was refluxed for 24 h. After the reaction, the mixture was cooled down, poured into EtOAc (20 mL), and filtered to remove the generated white solid. The combined EtOAc filtrates were concentrated in vacuo to give an oily solid, then adding a little methanol, white solid was generated, filtered, air dried and recrystallized in MeOH to give white solid 4. Yield 87%; 

m.p. 94-95 ºC;  

1H NMR (CDCl3, 400 MHz) δ 6.85 (m, 8H), 4.27 (s, 4H), 4.15 (s, 8H), 3.56 (s, 12H); 

IRν/cm-1 3067, 2993, 2951, 2921, 2888, 1748, 1596, 1509, 1173, 742, 706.



Journal of the Brazilian Chemical Society

Print version ISSN 0103-5053

J. Braz. Chem. Soc. vol.25 no.1 São Paulo Jan. 2014

http://dx.doi.org/10.5935/0103-5053.20130276 

ARTICLE

Structural study and fluorescent property of a novel organic microporous crystalline material


Zhao Cheng; Bingqin Yang*; Meipan Yang; Binglin Zhang
Key Laboratory of Synthetic and Natural Functional Molecule Chemistry of Ministry of Education, College of Chemistry and Materials Science, Northwest University, 710069 Xi'an, China



 TAKE A TOUR

 VLADIVOSTOK, RUSSIA

 


 Map of vladivostok

Vladivostok - Wikipedia, the free encyclopedia

https://en.wikipedia.org/wiki/Vladivostok
Vladivostok (Russian: Владивосток; IPA: [vlədʲɪvɐˈstok] ( listen), literally ruler of the East) is a city and the administrative center of Primorsky Krai, Russia, ...

Vladivostok - Wikipedia, the free encyclopedia

https://en.wikipedia.org/wiki/Vladivostok
Vladivostok (Russian: Владивосток; IPA: [vlədʲɪvɐˈstok] ( listen), literally ruler of the East) is a city and the administrative center of Primorsky Krai, Russia, ...

 


 

 


 



 
 


 



People taste traditional food to celebrate Nowruz Festival in Vladivostok, Russia, on March 22, 2014. Nowruz is a traditional festival which celebrates the ...















सुकून उतना ही देना प्रभू, जितने से जिंदगी चल जाये। औकात बस इतनी देना, कि औरों का भला हो जाये।
DRUG APPROVALS BY DR ANTHONY MELVIN CRASTO …..FOR BLOG HOME CLICK HERE

Join me on Linkedin

View Anthony Melvin Crasto Ph.D's profile on LinkedIn

Join me on Facebook FACEBOOK
Join me on twitterFollow amcrasto on Twitter
Join me on google plus Googleplus

 amcrasto@gmail.com

09b37-misc2b027LIONEL MY SON
He was only in first standard in school when I was hit by a deadly one in a million spine stroke called acute transverse mylitis, it made me 90% paralysed and bound to a wheel chair, Now I keep him as my source of inspiration and helping millions, thanks to millions of my readers who keep me going and help me to keep my son happy
सुकून उतना ही देना प्रभू, जितने से
जिंदगी चल जाये।
औकात बस इतनी देना,
कि औरों का भला हो जाये।
//////

 Special Olympics World Games 2015



No comments:

Post a Comment