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Tuesday, 25 July 2017

N-(1-adamantile)-4-chlorobenzamide ( NMR IS EASY)

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N-(1-adamantile)-4-chlorobenzamide
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EVEN MOM CAN TEACH U NMR
N-(1-Adamantile)-4-chlorobenzamide (7a): White solid (231 mg, 80%),

1H NMR(600 MHz, CDCl3): 7.71 (d, J = 8.22 Hz, 2H), 7.41 (d, J = 8.22 Hz, 2H), 6.36 (brs, 1H), 4.24 (d, J = 7.02 Hz, 1H), 2.04 (s, 2H), 1.90 (brs, 6H), 1.84 (d, J = 13.08 Hz, 2H), 1.78 (s, 2H), 1.71 (d, J = 12.84 Hz, 2H);

13C NMR(150 MHz, CDCl3): 165.5, 137.4, 133.7, 128.8, 128.2, 53.8, 37.4, 37.1, 32.1, 31.9, 27.2, 27.1.
HRESIMS calcd for C17H21ClNO [M+H]+ 290.1312, found 290.1301.
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1H AND 13C NMR PREDICT
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///////http://www.rsc.org/suppdata/c7/cy/c7cy00832e/c7cy00832e1.pdf